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HRID594753

反应详情

EQUATION

反应方程式

HRID 594753 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1cccc(-c2ncccn2)c1
HCID22630818

3-(Pyrimidin-2-yl)benzaldehyde

C11H8N2O

结构：COC(=O)CCCC(N)c1c(OC)ccc2ccccc12
HCID69082274

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2ccccc2c1C1CCCC(=O)N1Cc1cccc(-c2ncccn2)c1
HCID69085224

未命名化合物

PROCEDURE

实验过程

Prepared according to general procedure 1 (GP1) using methyl 5-amino-5-(2-methoxynaphthalen-1-yl)pentanoate and commercially available 3-(pyrimidin-2-yl)benzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.84 min.; [M+H]+: 424.10 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound