HRID595339

反应详情

EQUATION

反应方程式

HRID 595339 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The (1S)-2-nitro-1-[3-({3-[(phenylmethyl)oxy]propyl}oxy)phenyl]ethanol in ethanol solution (8 g in 160 mL) was hydrogenated using a Pd (4%)/Pt(1%)/C catalyst (1.6 g). Upon consumption of the starting material and the hydroxylamine intermediate, the reaction product in ethanol was filtered.

WORKUP

后处理

  1. customUpon consumption of the starting material
  2. filtrationthe hydroxylamine intermediate, the reaction product in ethanol was filtered