HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoprene → Isoprene acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoprene | HCID 6557 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Product | Isoprene acrylonitrile | HCID 168239 | — |
Reaction Steps
Then, was added thereto 68.2 parts of isoprene and 1.79 parts of 2-chloropropionitrile as an organic halide, followed by stirring at 80° C. to conduct a polymerization reaction. After 114 hours, the same post-treatment as in Example 1 was carried out to give a random (isoprene/acrylonitrile) copolymer. The conversion rate of isoprene was 62% and the conversion rate of acrylonitrile was 64%. The analysis results of the random (isoprene/acrylonitrile) polymer obtained are shown in Table 5. The polymer was confirmed to have a chlorine atom at the terminal of the polymer chain.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09243100B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-7ce0d575ec9a4b12a3d83eb3451ddfcf |
| Source note | uspto-grants-2016_01 |