3-Chloro-2-methyl-1-propene → HCID 125476811, compound

HRID 595629Notes

Reaction equation

HRID 595629 reaction equation
Br[CH2:2][CH:3]=[CH:4][CH3:5].C(Cl)[C:7](=[CH2:9])[CH3:8]>>[CH3:5]/[CH:4]=[CH:3]/[CH2:2][C:2]#[C:3][CH2:4][CH2:5][CH2:8][CH2:7][CH3:9]

Participants

3

Reactant 2

HCID 112413-Chloro-2-methyl-1-propeneHCID 1224142-Butene, 1-bromo-

Product 1

HCID 125476811HCID 125476811, compound

Procedure

Obtained in 74% yield (as a 92:8 E/Z mixture) from 1-heptyn using 1-bromo-but-2-en and using methallylchloride according to the procedure described under a).

Sources & evidence

ORD record
ord-89a5805f424841d4ba73aeb58496b508
Source dataset
uspto-grants-2016_01
Patent number
US09243210B2

Reaction notes

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