HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isophorone → Beta-Isophorone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isophorone | HCID 6544 | — |
| Reactant | Triethanolamine | HCID 7618 | — |
| Product | Beta-Isophorone | HCID 10108 | — |
Reaction Steps
A mixture of 500 g of 3,3,5-trimethyl-cyclohex-5-en-1-one (isophorone) and 50 g of triethanolamine was refluxed for 4 hours, whereupon it was fractionally distilled to give a fraction at b.p. 170°. The isomerization was performed in a reaction vessel equipped with a lateral distillation column having the following characteristics:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04010205 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-546893ad79ed44788e1566a97905c226 |
| Source note | uspto-grants-1977_03 |