HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 20316894, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 20316891 | HCID 20316891 | — |
| Product | HCID 20316894 | HCID 20316894 | — |
Reaction Steps
In a manner similar to that of Reference Example 4, 5.16 parts of 2-cyclobutylamino-5,6-dimethoxy-3,4-dihydro-1(2H)-naphthalenone hydrochloride is hydrolyzed in a mixture of 75 volume parts 48 % hydrobromic acid and 15 volume parts acetic anhydride. The procedure yields 4 parts of 2-cyclobutylamino-5,6-dihydroxy-3,4-dihydro-1(2H)-naphthalenone hydrobromide. Melting point: 229°-240° C (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04010202 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-af386aaf20e54a229a8438debc2a9841 |
| Source note | uspto-grants-1977_03 |