Cyclohexanone → HCID 20316887, compound

HRID 596257Notes

Reaction equation

HRID 596257 reaction equation
[C:1]1(=O)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.Br.[NH2:9][CH:10]1[CH2:19][CH2:18][C:17]2[C:12](=[CH:13][CH:14]=[C:15]([OH:21])[C:16]=2[OH:20])[C:11]1=[O:22]>C(O)C>[C:1]1(=[N:9][CH:10]2[CH2:19][CH2:18][C:17]3[C:12](=[CH:13][CH:14]=[C:15]([OH:21])[C:16]=3[OH:20])[C:11]2=[O:22])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 7967CyclohexanoneHCID 12353616HCID 12353616, compound

Product 1

HCID 20316887HCID 20316887, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In a mixture of 50 volume parts of cyclohexanone and 200 volume parts of ethanol is dissolved 0.151 part of 2-amino-5,6-dihydroxy-3,4-dihydro-1(2H)-naphthalenone hydrobromide to produce 2-cyclohexylideneamino-5,6-dihydroxy-3,4-dihydro-1(2H)-naphthalenone.

Sources & evidence

ORD record
ord-e605b75452c54e3dbe43570f98626af7
Source dataset
uspto-grants-1977_03
Patent number
US04010202

Reaction notes

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