Allyl Alcohol → HCID 21451199, compound

HRID 596267Notes

Reaction equation

HRID 596267 reaction equation
ClCCC[O:5][P:6]1[CH2:10][CH:9]=[C:8]([CH3:11])[CH2:7]1.[CH2:12](O)[CH:13]=[CH2:14]>>[CH2:14]([P:6]1(=[O:5])[CH2:10][CH:9]=[C:8]([CH3:11])[CH2:7]1)[CH:13]=[CH2:12]

Participants

3

Reactant 2

HCID 7858Allyl AlcoholHCID 21451191HCID 21451191, compound

Product 1

HCID 21451199HCID 21451199, compound

Procedure

To 8 g. (0.0448 mole) of 1-(chloropropoxy)-3-methyl-3-phospholene there was added 2.9 g. (0.05 mole) of allyl alcohol. The mixture was allowed to stand at room temperature and then distilled under reduced pressure to remove volatile material. There was thus obtained 1-allyl-3-methyl-3-phospholene-1-oxide.

Workup

  1. customto stand at room temperature
  2. distillationdistilled under reduced pressure
  3. customto remove volatile material

Sources & evidence

ORD record
ord-974c4dd0cca3401198189eb5a87c8b08
Source dataset
uspto-grants-1977_03
Patent number
US04010209

Reaction notes

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