Thionyl Chloride → HCID 54430147, compound

Participants

Reaction Steps

The starting compound, 5-chloromethyl-2-phenyl benzo [d]-1,3-dioxole (nD25 = 1.597) was prepared by chlorination, with SOCl2, of 5-hydroxymethyl-2-phenyl benzo [d]-1,3-dioxole melting (K) at 75° C, itself prepared by reduction, with Li Al H4, of 5-carbomethoxy-2-phenyl benzo [d]-1,3-dioxole, B.P./0.05 mm = 155° to 157° C, nD25 = 1.583.

Provenance & Evidence