HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,6-Hexanediol → HCID 21452026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,6-Hexanediol | HCID 12374 | — |
| Reactant | HCID 19761990 | HCID 19761990 | — |
| Product | HCID 21452026 | HCID 21452026 | — |
Reaction Steps
The same type of separable flask as used in Example 29 was charged with 118g (1 mol) of 1,6-hexanediol and 332g (2 mols) of methyltetrahydrophthalic anhydride. Addition reaction was carried out 2 hours at 140° to 170° C, providing 442g of 2:1 adduct of methyltetrahydrophthalic acid-1,6-hexanediol having an acid value of 238.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04010289 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-1f5517c4bca846f583f3807c92144d81 |
| Source note | uspto-grants-1977_03 |