HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(5,5-ethylenedioxy-5H-dibenzo[a,d]cyclohepten-2-yl)propan-1-ol → 2-(5,5-ethylenedioxy-5H-dibenzo-[a,d]cyclohepten-2-yl)propionaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(5,5-ethylenedioxy-5H-dibenzo[a,d]cyclohepten-2-yl)propan-1-ol | HCID 21450001 | — |
| Catalyst | HCID 178418647 | HCID 178418647 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2-(5,5-ethylenedioxy-5H-dibenzo-[a,d]cyclohepten-2-yl)propionaldehyde | HCID 21450003 | 70% |
Reaction Steps
0.5 Gm. of 2-(5,5-ethylenedioxy-5H-dibenzo[a,d]cyclohepten-2-yl)propan-1-ol in 50 ml. of benzene, is refluxed for 6 hours with 4.0 gm. of silver carbonate on celite, prepared as described in Compt. Rendus. (1968) C, 267, 900a. The mixture is cooled and filtered and the solution evaporated to afford a 70% yield of 2-(5,5-ethylenedioxy-5H-dibenzo-[a,d]cyclohepten-2-yl)propionaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011243 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-1f0fff69352147fa84bbefad9095ba2d |
| Source note | uspto-grants-1977_03 |