HCID 178460151, compound → HCID 178460152, compound

HRID 596538Notes

Reaction equation

HRID 596538 reaction equation
[CH2:1]([O:4][NH:5][C:6](=[C:10]1[C:15](=[O:16])[CH2:14][C:13]([CH3:18])([CH3:17])[CH2:12][C:11]1=[O:19])[CH2:7][CH2:8][CH3:9])[CH:2]=[CH2:3]>O>[OH2:4].[CH2:1]([O:4][NH:5][C:6](=[C:10]1[C:11](=[O:19])[CH2:12][C:13]([CH3:18])([CH3:17])[CH2:14][C:15]1=[O:16])[CH2:7][CH2:8][CH3:9])[CH:2]=[CH2:3]

Participants

3

Reactant 1

HCID 178460151HCID 178460151, compound

Product 1

HCID 178460152HCID 178460152, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

2.65g of 2-[1-(allyloxyamino)butylidene]-5,5-dimethylcyclohexane-1,3-dione was added to 10ml of water and the mixture was vigorously stirred. After several minutes, the precipitate was filtered, washed with water and dried. White crystal having a melting point of 46°-47° C was obtained.

Workup

  1. waitAfter several minutes
  2. filtrationthe precipitate was filtered
  3. washwashed with water
  4. customdried
  5. customwas obtained

Sources & evidence

ORD record
ord-cea87b21fcee4fe7ab42ee83e00174cb
Source dataset
uspto-grants-1977_03
Patent number
US04011256

Reaction notes

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