HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3,5-Bis(benzyloxy)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3,5-Bis(phenylmethoxy)benzoic acid | HCID 99307 | — |
| Product | 3,5-Bis(benzyloxy)benzoyl chloride | HCID 10831869 | — |
Reaction Steps
167 g of 3,5-dibenzyloxybenzoic acid and 400 ml of redistilled thionyl chloride were refluxed on an oil bath for one hour. Excess thionyl chloride was distilled off at reduced pressure, and the remaining mass crystallized. The product was recrystallized from petroleum ether (B.p., 60°-85° C.) : M.P. 73°-74° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011258 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-2514216a18514283ba4a2868bceff69e |
| Source note | uspto-grants-1977_03 |