HuagongsheHuagongshe Chemistry Print Report · For research reference only
Heptane → Squalane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Heptane | HCID 8900 | — |
| Reactant | 2,6,10,15,19,23-Hexamethyltetracosane-10,15-diol | HCID 13643265 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Squalane | HCID 8089 | — |
Reaction Steps
In a 300 ml autoclave were placed 20 g of 2,6,10,15,19,23-hexamethyltetracosane-10,15-diol, 40 ml of n-heptane, 0.4 ml of acetic acid and 0.4 g of 5 % palladium on active carbon and the mixture was hydrogenated at 200° C under a hydrogen pressure of 100 kg/cm2 for 15 hours to give squalane quantitatively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011277 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-85adb1127216473eb13b0d25785b87d9 |
| Source note | uspto-grants-1977_03 |