HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Phenoxyethoxy)-2-nitroaniline → HCID 21450209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Phenoxyethoxy)-2-nitroaniline | HCID 20545456 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21450209 | HCID 21450209 | — |
Reaction Steps
A mixture of 1.8 g. of 4-(2-phenoxyethoxy)-2-nitroaniline and 0.3 g. of 5% of palladium-on-charcoal catalyst in 200 ml. of methanol is hydrogenated under ambient conditions. After the uptake of hydrogen is complete, the mixture is filtered and 1,2-diamino-4-(2phenoxyethoxy)benzene is isolated from the filtrate by evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011320 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-016772973b01437cba4c35dbc361dba4 |
| Source note | uspto-grants-1977_03 |