HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 4-Chlorobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Trimethylsulfonium iodide | HCID 75127 | — |
| Reactant | 4-Chlorostyrene oxide | HCID 197010 | — |
| Product | 4-Chlorobenzaldehyde | HCID 7726 | — |
Reaction Steps
Following the procedure of Example 13 and employing 42.0 g. of 57% sodium hydride/mineral oil, 200 g. (1.0 mol) of trimethylsulfonium iodide and 70.4 g. (0.50 mol) of p-chlorobenzaldehyde there is obtained p-chlorostyrene oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011319 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-e6501dc02a664757ab99c62681875531 |
| Source note | uspto-grants-1977_03 |