HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 4-Methylbenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Trimethylsulfonium iodide | HCID 75127 | — |
| Reactant | 2-(4-Methylphenyl)oxirane | HCID 108111 | — |
| Product | 4-Methylbenzaldehyde | HCID 7725 | — |
Reaction Steps
Following the procedure of Example 16 and employing 4.84 g. (0.115 mol) of 57% sodium hydride, 23.5 g. (0.115 mol) of trimethylsulfonium iodide and 11.9 g. (0.099 mol) of p-tolualdehyde there is obtained p-methylstyrene oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011319 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-ce3b0e439ac74242961d69c2ea8aed9f |
| Source note | uspto-grants-1977_03 |