HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Methyltyramine → HCID 21406681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Methyltyramine | HCID 4657 | — |
| Reactant | (+-)-Methyl mandelate | HCID 78066 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 21406681 | HCID 21406681 | — |
Reaction Steps
A mixture of 20.0 g. (0.133 mol) of 4-methoxyphenylethylamine and 22.0 g. (0.133 mol) of methyl mandelate is heated at about 90° C. with stirring under nitrogen for 16 hours. The reaction mixture is taken up in ether and the product crystallized, giving N-[2-(4-methoxyphenyl)ethyl]mandelamide, m.p. 86°-88° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011319 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-69480ea4ea714cba96b741247e0ddcea |
| Source note | uspto-grants-1977_03 |