HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → 5-Tetradecyloxy-2-thiophenecarboxylic acid sodium salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 5-(Tetradecyloxy)thiophene-2-carboxylic acid | HCID 12361510 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 5-Tetradecyloxy-2-thiophenecarboxylic acid sodium salt | HCID 68117603 | — |
Reaction Steps
To 20.4 g (0.06 mole) of 5-tetradecyloxy-2-thiophenecarboxylic acid in 500 ml of methanol is added 5.4 g (0.10 mole) of sodium methoxide. The mixture is refluxed, and the methanol is distilled off being replaced by water. The aqueous solution is cooled, the precipitate collected, and dried to give 5-tetradecyloxy-2-thiophenecarboxylic acid sodium salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011333 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-dd220ed6d64c43cbaa65dc0a66cc289b |
| Source note | uspto-grants-1977_03 |