HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromomethyl 4-methoxyphenyl ketone → 4-Tert-butyl-1-(2-oxo-2-phenylethyl)pyridinium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromomethyl 4-methoxyphenyl ketone | HCID 4965 | — |
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | 4-tert-Butylpyridine | HCID 19878 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 4-Tert-butyl-1-(2-oxo-2-phenylethyl)pyridinium bromide | HCID 22462637 | — |
Reaction Steps
Employing the procedure of Example I above but replacing 4-methoxyphenacyl bromide with a substantially equimolecular amount of phenacyl bromide and replacing pyridine with a substantially equimolecular amount of 4-tert.butylpyridine there is obtained N-(phenacyl) 4-tert.butylpyridinium bromide, a white solid melting at 247-248° C., and which is soluble in water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029153 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-959a8d7f5df943bf90aac45c9708ec83 |
| Source note | uspto-grants-1977_03 |