HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanopyridine → N-(4-nitrophenacyl) 4-cyanopyridinium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanopyridine | HCID 7506 | — |
| Reactant | 2-Bromo-4'-nitroacetophenone | HCID 66840 | — |
| Reactant | 2-Chloro-1-(4-nitrophenyl)ethanone | HCID 264291 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | N-(4-nitrophenacyl) 4-cyanopyridinium chloride | HCID 86734538 | — |
Reaction Steps
Employing the procedure of Example III but replacing pyridine with a substantially equimolecular amount of 4-cyanopyridine and replacing 4-nitrophenacyl bromide with a substantially equimolecular amount of 4-nitrophenacyl chloride there is obtained N-(4-nitrophenacyl) 4-cyanopyridinium chloride, a white solid soluble in water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029153 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-0e6fb18cb8634602a19f282ad5c7cc00 |
| Source note | uspto-grants-1977_03 |