HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-4'-nitroacetophenone → N-(4-cyanophenacyl) 5-chloropyrimidinium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-4'-nitroacetophenone | HCID 66840 | — |
| Reactant | Benzonitrile, 4-(chloroacetyl)- | HCID 142493 | — |
| Reactant | 5-Chloropyrimidine | HCID 12600384 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | N-(4-cyanophenacyl) 5-chloropyrimidinium chloride | HCID 86734541 | — |
Reaction Steps
Employing the procedure of Example III but replacing 4-nitrophenacyl bromide with a substantially equimolecular amount of 4-cyanophenacyl chloride and replacing pyridine with a substantially equimolecular amount of 5-chloropyrimidine there is obtained N-(4-cyanophenacyl) 5-chloropyrimidinium chloride, a solid soluble in water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029153 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-544e910fdfe04417ad05742fc5dce802 |
| Source note | uspto-grants-1977_03 |