2-Chloro-N,N-dimethylethylamine → HCID 86733023, compound

HRID 596859Notes

Reaction equation

HRID 596859 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:18]=[CH:19][C:20]=1[Cl:21])[CH2:5][N:6]1[CH2:11][CH2:10][NH:9][CH2:8][CH:7]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.[CH2:22]([N:24]([CH2:27]CCl)[CH2:25]C)[CH3:23].CN(CCCl)C>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:18]=[CH:19][C:20]=1[Cl:21])[CH2:5][N:6]1[CH2:11][CH2:10][N:9]([CH2:23][CH2:22][N:24]([CH3:27])[CH3:25])[CH2:8][CH:7]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

4

Reactant 3

HCID 79012-Chloro-N,N-dimethylethylamineHCID 13364Diethylaminoethyl chlorideHCID 21448557HCID 21448557, compound

Product 1

HCID 86733023HCID 86733023, compound

Procedure

1-(3',4'-Dichloro benzyl)-2-phenyl piperazine prepared according to Example 3 (b), is alkylated by following the procedure described in Example 3 (c), whereby, in place of the diethylamino ethylchloride, the equimolecular amount of dimethylamino ethylchloride is used. The resulting reaction product is obtained in the form of a light yellow oil boiling at 190° C./0.01 mm. Hg.

Workup

  1. customThe resulting reaction product

Sources & evidence

ORD record
ord-4d8e259aab3d4b7fb21311533d7aff08
Source dataset
uspto-grants-1977_03
Patent number
US04012389

Reaction notes

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