Diethylaminoethyl chloride → HCID 54042764, compound

HRID 596861Notes

Reaction equation

HRID 596861 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:18]=[CH:19][C:20]=1[Cl:21])[CH2:5][N:6]1[CH2:11][CH2:10][NH:9][CH2:8][CH:7]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C(N(CCCl)CC)C.[CH2:30]([N:32]([CH2:35][CH2:36][CH2:37]Cl)[CH2:33][CH3:34])[CH3:31]>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:18]=[CH:19][C:20]=1[Cl:21])[CH2:5][N:6]1[CH2:11][CH2:10][N:9]([CH2:37][CH2:36][CH2:35][N:32]([CH2:33][CH3:34])[CH2:30][CH3:31])[CH2:8][CH:7]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

4

Reactant 3

HCID 13364Diethylaminoethyl chlorideHCID 669183-Chloropropyl(diethyl)amineHCID 21448557HCID 21448557, compound

Product 1

HCID 54042764HCID 54042764, compound

Procedure

1-(3',4'-Dichloro benzyl)-2-phenyl piperazine prepared according to Example 2 (b), is alkylated by following the procedure described in Example 2 (c) whereby, in place of the diethylamino ethylchloride, the equimolecular amount of diethylamino propylchloride is used. The resulting reaction product is obtained in the form of a light yellow oil boiling at 210° C./0.04 mm. Hg.

Workup

  1. customThe resulting reaction product

Sources & evidence

ORD record
ord-de879dd0307d4c898a895b1adaf7e612
Source dataset
uspto-grants-1977_03
Patent number
US04012389

Reaction notes

Loading…