Diethylaminoethyl chloride → HCID 54566101, compound

HRID 596862Notes

Reaction equation

HRID 596862 reaction equation
[CH2:1]([O:8][C:9]1[CH:27]=[CH:26][C:12]([CH2:13][N:14]2[CH2:19][CH2:18][NH:17][CH2:16][CH:15]2[C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:28]([N:30]([CH2:33][CH2:34]Cl)[CH2:31][CH3:32])[CH3:29]>>[CH2:1]([O:8][C:9]1[CH:27]=[CH:26][C:12]([CH2:13][N:14]2[CH2:19][CH2:18][N:17]([CH2:29][CH2:28][N:30]([CH2:33][CH3:34])[CH2:31][CH3:32])[CH2:16][CH:15]2[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=2)=[CH:11][CH:10]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 13364Diethylaminoethyl chlorideHCID 21448563HCID 21448563, compound

Product 1

HCID 54566101HCID 54566101, compound

Procedure

1-(4'-Benzyloxy benzyl)-2-phenyl piperazine prepared according to Example 10, is alkylated by means of diethylamino ethylchloride by following the procedure described in Example 2 (c). The resulting reaction product is obtained in the form of a light yellow oil boiling at 235° C./0.01 mm. Hg.

Workup

  1. customThe resulting reaction product

Sources & evidence

ORD record
ord-23b56e2c9d494f5e95821920af4655e9
Source dataset
uspto-grants-1977_03
Patent number
US04012389

Reaction notes

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