HRID596895
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Alternatively 4-(3',4'-diethylphenyl) butanoic acid (23.3 g; 0.106 mole) maybe cyclised by stirring at 100° C with 80% sulphuric acid (115 ml) for 11/2 hours. After dilution, extraction into ether, and distillation 15.83 g (74%) of the tetralone was obtained.
WORKUP
后处理
- extractionAfter dilution, extraction into ether
- distillationdistillation 15.83 g (74%) of the tetralone
- customwas obtained