HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178422544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 10540931 | HCID 10540931 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178422544 | HCID 178422544 | — |
Reaction Steps
3-Cyano-7-methylthioxanthone-10,10-dioxide (0.36 g), sodium azide (0.091 g), ammonium chloride (0.081 g) and dimethyl formamide (5.0 ml) were heated together on the steam bath for 7 hrs., poured on to ice and hydrochloric acid, and the precipitated tetrazole filtered off, washed with water and recrystallised from acetic acid, m.p. 267° C (decomposes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04012499 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-c1c5e99e0e8142a9b598a3db241e767f |
| Source note | uspto-grants-1977_03 |