HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 21449486, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 21449481 | HCID 21449481 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21449486 | HCID 21449486 | — |
Reaction Steps
(1-Hydroxy-2-isopropyl-2-methyl-6,7-dichloro-5-indanyloxy)acetic acid is prepared following substantially the same procedure described in Example 4, Step F, using the following substances: 2-methyl-2-isopropyl-6,7-dichloro-1,5-indandiol (8.3 g., .03 mole); potassium carbonate (7.2 g.); ethyl bromoacetate (6.2 ml.); and dimethylformamide (70 ml.); and hydrolyzing the resultant ester with aqueous sodium hydroxide in accordance with Example 4, Step F, gives (1-hydroxy-2-isopropyl-2-methyl-6,7-dichloro-5-indanyloxy)acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04012524 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-b5dd016fec07417d8d22450f4592be38 |
| Source note | uspto-grants-1977_03 |