HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → 1H-1,4-Benzodiazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | 1,4Benzodiazepine-1-acetamide | HCID 23201858 | — |
| Product | 1H-1,4-Benzodiazepine | HCID 148431 | — |
Reaction Steps
In the manner given in Example 1, N,N-dimethyl-8-chloro-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4benzodiazepine-1-acetamide is reduced with borane to give 1-[2-(dimethylamino)ethyl]-8-chloro-5,6-dihydro-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4-benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04012413 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-e0395511b599499fbaf3969958104e68 |
| Source note | uspto-grants-1977_03 |