HuagongsheHuagongshe Chemistry Print Report · For research reference only
M-Cresol → HCID 22105127, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | M-Cresol | HCID 342 | — |
| Reactant | Cyclopentene | HCID 8882 | — |
| Product | HCID 22105127 | HCID 22105127 | 19.9% |
Reaction Steps
130 g of cyclopentene are added dropwise to 108 g of m-cresol and 10 g of an acid-activated fuller's earth at 140° C. The mixture is stirred at this temperature for 1 h. After removal of the catalyst by filtration the mixture is fractionated. 35 g of 3-methyl-6-cyclopentylphenol boiling at 113° C (1.4 mm Hg) are obtained. A further fraction (112 g) boiling at 154° C (0.9 mm Hg) consists of 3-methyl-4,6-dicyclopentylphenol (melting point: 45° C).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04013473 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-1e8603e7f0974b44a18d3b56552e7868 |
| Source note | uspto-grants-1977_03 |