HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → 2,6-Dicyclopentyl-3,5-xylenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 3,5-Dimethylphenol | HCID 7948 | — |
| Reactant | Cyclopentene | HCID 8882 | — |
| Product | 2,6-Dicyclopentyl-3,5-xylenol | HCID 6454047 | 656.4% |
Reaction Steps
700 g of cyclopentene are added dropwise to 610 g of 3,5-dimethylphenol and 60 g of p-toluene sulphonic acid at 120° C. The catalyst is removed by washing with sodium hydrogen carbonate solution. The mixture is fractionated. At boiling point 141° C (0.6 mm Hg) 591 g of 3,5-dimethyl-2,6-dicyclopentylphenol are obtained. Melting point: 69° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04013473 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-fb1d2327e58a429dab3a4d4a36f9123a |
| Source note | uspto-grants-1977_03 |