HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethoxy-1-(ethoxycarbonyl)-1,2-dihydroquinoline → HCID 20381764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethoxy-1-(ethoxycarbonyl)-1,2-dihydroquinoline | HCID 27833 | — |
| Reactant | HCID 20381778 | HCID 20381778 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20381764 | HCID 20381764 | — |
Reaction Steps
A solution of 1.5g of 3-[o-aminophenoxy]-indole-2-carboxylic acid in 50ml of THF was treated with 1.48g of EEDQ and the clear solution left 18 hours at ambient temperature. The THF was removed by distillation, and the residue was rubbed with 2N HCl to give a yellow solid. Recrystallization from ethanol gave analytical material, mp. 233°-4°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04013641 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-94f00e068a234b5180bf6f109633ef22 |
| Source note | uspto-grants-1977_03 |