Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Benzene, 1,1′-[1-(chloromethyl)-1,2-ethenediyl]bis- | HCID 54379748 | — |
| Product | HCID 70638196 | HCID 70638196 | — |
Reaction Steps
A solution consisting of 4 parts of 2,3-diphenylallyl chloride dissolved in 7.12 parts of diethylamine is allowed to stand at 65° for about 24 hours. Then the excess diethylamine is removed under nitrogen and the oil and solid which remain are covered with n-hexane. The solid is separated by filtration and the filtrate is acidified by adding isopropanolic hydrochloric acid. The oil which separates is then isolated by decantation and crystallized from isopropanol-ethyl ether to yield pure N,N-diethyl-2,3-diphenylallylamine hydrochloride, melting at about 190° and displaying maxima in the nuclear magnetic resonance spectrum at about 70, 76, 82, 162-190, 242, 246 and 422-436 Hertz. That compound is represented by the following structural formula ##STR4##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04013643 |
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| Source dataset | uspto-grants-1977_03 |
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| ORD ID | ord-83aafe142f3e43428908bc9576720777 |
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| Source note | uspto-grants-1977_03 |
|---|
