1-Methyl-4-piperidone → HCID 20304672, compound

HRID 597169Notes

Reaction equation

HRID 597169 reaction equation
[ClH:1].N[N:3]1[C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=2[CH2:7][O:6][CH2:5][CH2:4]1.[CH3:14][N:15]1[CH2:20][CH2:19][C:18](=O)[CH2:17][CH2:16]1>>[ClH:1].[CH3:14][N:15]1[CH2:20][CH2:19][C:18]2[N:3]3[C:9]4[C:10](=[CH:11][CH:12]=[CH:13][C:8]=4[CH2:7][O:6][CH2:5][CH2:4]3)[C:17]=2[CH2:16]1

Participants

3

Reactant 2

HCID 740491-Methyl-4-piperidoneHCID 20304799HCID 20304799, compound

Product 1

HCID 20304672HCID 20304672, compound

Procedure

By a procedure similar to that described in Example 110, 1-amino-1,2,3,5-tetrahydro-4,1-benzoxazepine hydrochloride is reacted with 1-methyl-4-piperidone to yield the title compound, m.p. 286°-288° .

Sources & evidence

ORD record
ord-5880d1ada49c463ea91d7662d64aed7a
Source dataset
uspto-grants-1977_03
Patent number
US04013652

Reaction notes

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