HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 3,5-Diphenyl-1H-pyridazin-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 4-(Diethylamino)-1,3-diphenylbut-3-ene-1,2-dione | HCID 53932832 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 3,5-Diphenyl-1H-pyridazin-4-one | HCID 619203 | — |
Reaction Steps
The product solution from Example 1 was cooled to 0° C. and mixed with 20 ml. of isopropyl alcohol and 2 ml. of hydrazine. The mixture was stirred for 10 minutes, and was then warmed to room temperature and stirred for 15 hours. The product was then collected by filtration. The yield was 6.0 g. of 3,5-diphenyl-4(1H)-pyridazinone, m.p. 328°-32° C., which was identified by infrared and nuclear magnetic resonance analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04013658 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-a361d087769a4d7d99e2c6a35a6653cd |
| Source note | uspto-grants-1977_03 |