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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 597188Generated: October 31, 2026

Phosphorus pentachloride → HCID 21446964, compound

https://huagongshe.com/reaction/597188

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhosphorus pentachlorideHCID 24819—
Reactant1-MethylpiperazineHCID 53167—
ReactantHCID 20381773HCID 20381773—
ProductHCID 21446964HCID 21446964—

Reaction Steps

In the same way as described in example 1, 3-chloro-7-methyl-7H-indolo[3,2-b][1,5]benzoxazepine-6(5H)-one, phosphorous pentachloride and N-methyl piperazine were reacted. The solid product was recrystallized from ethanol for analysis, mp. 187°-8°.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04013660
Source datasetuspto-grants-1977_03
ORD IDord-be7839377df24131960c871f158fc333
Source noteuspto-grants-1977_03