HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12772994, compound → HCID 22749073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12772994 | HCID 12772994 | — |
| Solvent | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Product | HCID 22749073 | HCID 22749073 | — |
Reaction Steps
A solution of 1-(p-chlorobenzamido)pyridinium internal salt (20 parts) in p-chlorobenzoyl chloride was allowed to stand for 2 hours at 25° C. The crystalline solid which formed was filtered off, washed and dried to give 1-(bis(p-chlorobenzoyl) amino)pyridinium chloride (20 parts), melting point 195° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04013669 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-6dcf21e1570f4687bda1f30d7becb37c |
| Source note | uspto-grants-1977_03 |