HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 70609976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | (3-Phenylcyclopenta[b]pyran-2-yl)acetonitrile | HCID 70638352 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 70609976 | HCID 70609976 | — |
Reaction Steps
As an illustration of an acid hydrolysis of nitrile intermediates a mixture of 5 g. of 3-phenyl-7-benzofuranacetonitrile in 30 ml. of acetic acid, 20 ml. of water and 20 ml. of sulfuric acid is stirred and heated at reflux overnight. On cooling and diluting with water one obtains 3-phenyl-7-benzofuranacetic acid, purified by crystallization from benzenehexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04013692 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-6f0ceab83c5c43df973bbd7ad6d68ffd |
| Source note | uspto-grants-1977_03 |