Phenol, 3-cyclohexyl- → HCID 21447455, compound

HRID 597303Notes

Reaction equation

HRID 597303 reaction equation
[CH:1]1([C:7]2[CH:8]=[C:9]([OH:13])[CH:10]=[CH:11][CH:12]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C([O:16][C:17](=[O:22])[CH2:18][CH2:19][CH2:20]Br)C>CCCCCC>[CH:1]1([C:7]2[CH:8]=[C:9]([CH:10]=[CH:11][CH:12]=2)[O:13][CH2:20][CH2:19][CH2:18][C:17]([OH:22])=[O:16])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

Participants

4

Reactant 2

HCID 16036Phenol, 3-cyclohexyl-HCID 76300Ethyl 4-bromobutyrate

Product 1

HCID 21447455HCID 21447455, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Following an analogous procedure to that described in Examples 1 and 2, m-cyclohexylphenol and 4-bromobutyric acid ethyl ester give 4-(m-cyclohexylphenoxy)-butyric acid of melting point 83° -84° C (from hexane).

Sources & evidence

ORD record
ord-c31977b479b241028f49cad5f4156344
Source dataset
uspto-grants-1977_03
Patent number
US04013708

Reaction notes

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