HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(1-Adamantyl)phenol → 4-[4-(1-Adamantyl)-phenoxy]-crotonic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(1-Adamantyl)phenol | HCID 269933 | — |
| Reactant | Ethyl (E)-4-bromobut-2-enoate | HCID 5373944 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-[4-(1-Adamantyl)-phenoxy]-crotonic acid ethyl ester | HCID 70637851 | — |
Reaction Steps
Analogously to the procedure described in Example 5, the use of 11.4 g of 4-(1-adamantyl)-phenol and 14.5 g of 4-bromocrotonic acid ethyl ester as starting materials gives 4-[4-(1-adamantyl)-phenoxy]-crotonic acid ethyl ester of melting point 91°-93° C (from methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04013719 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-df8b52f88d3b49048a0ffe9ee0518686 |
| Source note | uspto-grants-1977_03 |