HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → HCID 53885077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | HCID 21445118 | HCID 21445118 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53885077 | HCID 53885077 | 45.8% |
Reaction Steps
60 g of 3,3-dimethoxy-hexananilide were heated at 145° C until the distillation of methanol ceased and after cooling, isopropyl ether was added thereto. The precipitate formed was recovered by vacuum filtration to obtain 24 g of 3-methoxy-2-hexenanilide melting at 104° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04014679 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-dd1b4716b664486f8efa3945ef996789 |
| Source note | uspto-grants-1977_03 |