HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 6-Nitroveratrylidenecyclohexylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | 6-Nitroveratraldehyde | HCID 88505 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 6-Nitroveratrylidenecyclohexylamine | HCID 54195554 | 80.4% |
Reaction Steps
A suspension of 42.2 g (0.2 mole) of 6-nitroveratraldehyde, 19.8 g (0.2 mole) cyclohexylamine, 1.0 ml. glacial acetic acid, and 1.25 l. ethanol was stirred and refluxed for 5 min., cooled, and filtered. The solid was washed with 100 ml. cold ethanol and air dried to give 47.0 g (80%) of the product, m.p. 160°-161°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04014886 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-d4c4459d41c3462bb9b828a544d23a8b |
| Source note | uspto-grants-1977_03 |