HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 58522-71-7
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 6-Nitroveratraldehyde | HCID 88505 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 58522-71-7 | HCID 12439587 | 72.7% |
Reaction Steps
A suspension of 6-nitroveratraldehyde (84 g, 0.4 mole), 600 ml of ethanol, and 1 ml of acetic acid was refluxed with 2-methoxyethylamine (30 g, 0.44 mole) for 1.5 hrs. After cooling overnight filtration gave 78 g of the product; m.p. 65°-66°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04014886 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-e1cf4bc4ba814fa5983ab4b786e50930 |
| Source note | uspto-grants-1977_03 |