HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 1-Oxaspiro[4.5]decan-6-ol, 2,6,10,10-tetramethyl-, 6-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 6-Hydroxydihydrotheaspirane | HCID 65428 | — |
| Product | 1-Oxaspiro[4.5]decan-6-ol, 2,6,10,10-tetramethyl-, 6-acetate | HCID 93838 | — |
| Product | HCID 23346561 | HCID 23346561 | — |
Reaction Steps
2,6,10,10-Tetramethyl-1-oxa-spiro[4.5]dec-6-yl acetate was prepared as indicated hereinabove, from 2,6,10,10-tetramethyl- 1-oxa-spiro[4.5]decan-6-ol and acetyl chloride. 2,6,10,10-Tetramethyl-1-oxa-spiro[4.5]dec-6-yl formate on the contrary was obtained by treating the above alcohol with formylimidazole, according to the method given in Liebigs Ann. Chem. 655, 95 (1962).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04014905 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-64a6f52819a54718ba21714b865e3195 |
| Source note | uspto-grants-1977_03 |