HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 3-Cyclopropylpropyl 10,12-tetradecadienoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 3-Cyclopropylpropan-1-ol | HCID 20426485 | — |
| Reactant | 10,12-Tetradecadien-1-oyl chloride | HCID 53805337 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 3-Cyclopropylpropyl 10,12-tetradecadienoate | HCID 54542540 | — |
Reaction Steps
To 30 ml. anhydrous ether and 0.23 g. 10,12-tetradecadien-1-oyl chloride is added 0.1 g. 3-cyclopropyl-1-propanol. The mixture is cooled to 0° and 0.5 ml. pyridine is added. The reaction mixture is stirred for 1 day at room temperature and then is worked up following the procedure of Example 3 to yield 3-cyclopropylpropyl 10,12-tetradecadienoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04014922 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-0d43f175255046fa85909f97af7037e8 |
| Source note | uspto-grants-1977_03 |