HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-formylphenyl)acetamide → HCID 76168095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-formylphenyl)acetamide | HCID 256849 | — |
| Reactant | 3,5-Diacetyl-2,6-dihydroxy-4h-pyran-4-one | HCID 135465969 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 76168095 | HCID 76168095 | — |
Reaction Steps
Similarly, 4.2 g. (0.02 m.) of 3,5-diacetyl-4,6-dihydroxy-2H-pyran-2-one, 3.2 g. (0.02 m.) of m-acetamidobenzaldehyde, 200 ml. of chloroform and 0.5 ml. of piperidine is azeotroped for four hours and the reaction mixture is filtered to yield 3-(m-acetamidocinnamoyl)-5-acetyl-4-hydroxy-2H-pyran-2,6(3H)-dione, m.p. 222°-224° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04015009 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-d32d1a58661b438a95399c91da2c3ce0 |
| Source note | uspto-grants-1977_03 |