Pyridine → HCID 54118725, compound

HRID 597742Notes

Reaction equation

HRID 597742 reaction equation
[C:1]1([CH:7]=[C:8]([C:21]2[CH:26]=[CH:25][C:24]([O:27]C)=[C:23]([O:29]C)[C:22]=2[O:31]C)[C:9]2[CH:14]=[CH:13][C:12]([O:15]C)=[C:11]([O:17]C)[C:10]=2[O:19]C)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.N1C=CC=CC=1>O>[C:1]1([CH:7]=[C:8]([C:9]2[CH:14]=[CH:13][C:12]([OH:15])=[C:11]([OH:17])[C:10]=2[OH:19])[C:21]2[CH:26]=[CH:25][C:24]([OH:27])=[C:23]([OH:29])[C:22]=2[OH:31])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 1049PyridineHCID 54152640HCID 54152640, compound

Product 1

HCID 54118725HCID 54118725, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The product of Example 9 was heated under reflux with pyridine chlorhydrate for 10 minutes then the reaction mixture was added to water. On recrystallisation of the resulting precipitate from a mixture of water and alcohol, crystals of 1-phenyl-2,2-di-(2,3,4-trihydroxyphenyl) ethylene having a melting point of 142° - 143° C were obtained. ##STR10##

Workup

  1. customOn recrystallisation of the resulting precipitate
  2. additionfrom a mixture of water and alcohol, crystals of 1-phenyl-2,2-di-(2,3,4-trihydroxyphenyl) ethylene having a melting point of 142° - 143° C
  3. customwere obtained

Sources & evidence

ORD record
ord-782eb3a1c2074105b629fc54eb4af188
Source dataset
uspto-grants-1977_03
Patent number
US04015017

Reaction notes

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