HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfanium bromide → Sulfonium perfluorobutane sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfanium bromide | HCID 23498378 | — |
| Reactant | Sodium perfluorobutanesulfonate | HCID 23678450 | — |
| Solvent | Nitromethane | HCID 6375 | — |
| Product | Sulfonium perfluorobutane sulfonate | HCID 22483813 | — |
Reaction Steps
The thus obtained monomer precursor is mixed with, for example, phenacyl bromide in acetonitrile or nitromethan at room temperature, to thereby obtain the corresponding sulfonium bromide. With the thus obtained sulfonium bromide, for example, sodium perfluorobutane sulfonate is mixed in nitromethane at room temperature to thereby obtain the targeted product of sulfonium perfluorobutane sulfonate. Moreover, the thus obtained sulfonium perfluorobutanesulfonate can be further purified by recrystallization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897321B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-b7f149b3e99a4d5aabb5b4e532189636 |
| Source note | uspto-grants-2011_03 |