HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 597758Generated: October 30, 2026
Glycidyl methacrylate → 1,2-Dihydroxy-3-[4'-(di-p-tolylamino)stilbene-4-yloxy]propane
https://huagongshe.com/reaction/597758
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Glycidyl methacrylate | HCID 7837 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-(2-{4-[Bis(4-methylphenyl)amino]phenyl}ethenyl)phenol | HCID 59922671 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 1,2-Dihydroxy-3-[4'-(di-p-tolylamino)stilbene-4-yloxy]propane | HCID 57977102 | — |
Reaction Steps
In a reaction vessel equipped with a stirrer, a thermometer, a condenser, and a dropping funnel, 11.75 g of 4-hydroxy-4′-(di-p-tolylamino)stilbene, 4.35 g of glycidyl methacrylate, and 8 ml of toluene are contained, and the mixture is heated to 90° C. Further, 0.16 g of triethylamine is added thereto, and the mixture is agitated for 8 hours at 95° C. Next, 16 ml of toluene and 20 ml of a 10% aqueous solution of sodium hydroxide are added thereto, and the mixture is further agitated for 8 hours at 95° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07897313B2 |
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| Source dataset | uspto-grants-2011_03 |
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| ORD ID | ord-6a4acced500b4708ad0f9ec8c3a98ab6 |
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| Source note | uspto-grants-2011_03 |
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