HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 67270933, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-(4-Chlorophenyl)but-3-yn-2-amine | HCID 15841029 | — |
| Catalyst | Lindlars catalyst | HCID 131709914 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 67270933 | HCID 67270933 | 98.3% |
Reaction Steps
A mixture of 3-(4-chloro-phenyl)-1-methyl-prop-2-ynylamine (1.5 g, 8.4 mmol), triethylamine (0.12 mL, 0.86 mmol, 0.1 eq.) and Lindlar catalyst (150 mg) in 40 mL of 1:1 methanol-dichloromethane was stirred for 1 hr, filtered through a CELITE pad and concentrated to provide 1.5 g of 3-(4-chloro-phenyl)-1-methyl-allylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897601B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-050014eb15304e75b83d4bdca4b951da |
| Source note | uspto-grants-2011_03 |